NMR spectroscopy is extensively utilized across various disciplines of pharmaceutical research. The advancement of magnetic resonance technology has enabled diverse and high-resolution analyses. The importance of data from different sources in pharmaceutical research has increased. NMR spectroscopy is an effective pharmaceutical method with easy application and routine applicability. Another advantage of this method, which allows drug research not only from the chemical but also from the biological and biophysical aspects, is that it is marker-free. Initially utilized at a single level and primarily focused on specific elements such as chemical synthesis and structure-activity elucidation, NMR methodology has evolved to produce multi-level biomolecular and clinically relevant data, including metabolomics and 3D modelling, by integrating it with other instrumental techniques used in pharmaceutical sciences. From this perspective, NMR spectroscopy has found broader applications in pharmaceutical sciences. This section discusses pharmaceutical instrumentation methods combined with NMR technology, their importance, and current publications.